Course code:
1302P		 Course name:
Analytical Chemistry 2

Academic year:

2012/2013.

Attendance requirements:

There are no requirements.

ECTS:

10

Study level:

basic academic studies

Study program:

Chemistry Teacher: 2. year, winter semester, compulsory course

Teacher:

Rada M. Baošić, Ph.D.
full professor, Faculty of Chemistry, Studentski trg 12-16, Beograd

Assistants:

Ivanka Ž. Ćirić, Ph.D.
senior research associate, Innovation center, Studentski trg 12-16, Beograd

Nikola R. Stevanović, Ph.D.

Hours of instruction:

Weekly: two hours of lectures + one hour of exercises + six hours of labwork (2+1+6)

Goals:

Acquisition of basic knowledge of quantitative chemical analysis (gravimetry and volumetry); introduction to the procedures of sampling of representative samples; selecting and applying the most appropriate methods; and assessment approaches in the course of solving problems in the analysis of complex ie. real samples; achievement skills, accuracy and precision in work.

Outcome:

A student is qualified to choose the method for quantitative analysis of the corresponding sample and to make the determination with the required accuracy and precision.

Teaching methods:

Lectures, labwork (group and individual) and theoretical exercises.

Extracurricular activities:

Student writing group exercises, solves problems and elaborates the principles of analysis.

Coursebooks:

Main coursebooks:

  • ¨. Savić, ź. Savić: Fundamentals of analytical chemistry, Sarajevo
  • S. Mandić, R. Baošić, ¨. źutić: Practicum of Analytical chemistry 2

Supplementary coursebooks:

  • D. A. Skoog, D. M. West, F. J. Holler: Fundamentals of analytical chemistry, 1999.

Additional material:

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  Course activities and grading method

Lectures:

2 points (2 hours a week)

Syllabus:

  • Introduction, division.
  • Gravimetry; examples of determination.
  • Introduction in volumetry; division; titration curves; standard solutions; techniques.
  • Acid-base titration; titration curves; examples of determination.
  • Nonaqueous titrations.
  • Precipitation methods; titration curves; examples of determination.
  • Complexometry; titration curves; techniques; selectivity; application.
  • Redox methods; division; titration curves; formal potential; examples of determination.
  • Sampling and translation complex samples in solution.
  • Analysis of real sample.
  • Validation of obtained results.

Exercises:

3 points (1 hour a week)

Labwork:

38 points (6 hours a week)

Syllabus:

  • Gravimetry; individual analysis.
  • Group exercises from the methods of neutralization; individual analysis.
  • Group exercises from the methods of precipitation; individual analysis.
  • Group exercises from the complexometry; individual analysis.
  • Group exercises from the redox methods; individual analysis.

Written exam:

30 points

Oral exam:

27 points